Today’s brazing technology is based on a strong foundation of the brazing experiences of many people around the world over a period of many decades (even centuries). I’ve now been very active in the brazing world for almost 50-years, and, like my predecessors in the world of brazing, I’ve learned a lot about this fascinating joining process (and I’m still learning). In this article, I’d like to share with you one of my brazing experiences from many years back, one that involved high-temperature differential-expansion between an 18” (45 cm) diameter tool steel die and a thin carbide plate (round disc) that needed to be brazed to the die’s front surface for wear-protection.
When trying to braze together materials that have widely different Coefficients Of Thermal Expansions (COE’s), the material with the higher expansion rate (COE) will grow faster than the other when heated and shrink (contract) faster when cooled down from the brazing temperature. Once the two different materials have been brazed together and cooling begins, the shrinkage-rate differences between those two materials can produce significant shear stresses at the brazed interface between them. These stresses can, in some cases, be so strong that the thin brazed joint may be torn apart at either interface, or it might cause fracturing of either base metal, or perhaps open up a large crack through the BFM layer itself. It was this extreme — and very real — differential expansion problem that we had to address in today’s “history lesson”.
Shown in Fig. 1 is a photo of one of today’s modern plastic extrusion pelletizing dies, in which plastic is continuously extruded through the many small holes in the face of that small diameter die and cut into small pellets by a constantly rotating sharp cutter.
In the early 1980’s I was working on a brazing project for a client, a pelletizing company in New York State who made specialized high-temp extrusion dies with a unique rotating cut-off knife system. The overall process and unique application were confidential, so I’ll speak of it in general terms, but the brazing principles involved in making this “pelletizing” die assembly can be shared.
The extrusion die itself was a large diameter (18-inches/45 cm) tool-steel die, with many holes in its front face through which the end-use material was continuously extruded and cut off at a required length, all this being done at a high rate of speed. The rapidly rotating cutter, cutting the extruded product into about 15-in (40 cm) lengths, had a very sharp carbide cutting edge, which could quickly wear away the face of the tool steel die if that face were not protected by a very hard, wear-resistant surface. In our discussions with the client, we agreed to braze a large carbide disc onto the front of the tool steel die, which would significantly reduce the wear on the die surface.
In this particular case, the operating temp for this extrusion die was going to be high enough in temperature that the use of standard copper sheets between the carbide and die for the purpose of absorbing differential-expansion stresses between the die and the carbide could not be done, nor could low-temp silver-based brazing filler metals (BFMs) be used, even though the use of ductile pure copper sheets as a stress-reducing layer between the carbide and the die, and the use of silver-based BFMs to keep the brazing temps low, were both commonly being used for making cutting-tools at that time (still widely used today). Since neither of these low-temp materials could effectively be used in this high-temp die application, we had to look at higher temp shock-absorber material (such as pure nickel) and high-temp BFMs (such as nickel-based BFMs).
The final product was made via high-temp nickel brazing in a vacuum furnace, using a pure nickel sheet (Nickel 200) as the “shock-absorber” to absorb the differential-expansion stresses we knew would be present in this application. This is illustrated in Fig. 2.
IMPORTANT — Note that the carbide disc in Fig. 2 had to be made from much smaller pie-shaped carbide segments since a much larger solid disc of carbide would not have worked (it had been tried) because of the significant difference in COE’s between the carbide and the tool steel used for the die.
Assembly and brazing procedures.
The die face was machined flat. The carbide pieces, too, were very flat, and cut into close-fitting pie shapes. The carbide pieces were about 3/8” (10mm) thick and were carefully matched for a good fit, with a close, parallel gap-clearance between each one, so that the molten BFM could flow nicely into and through each joint in the carbide assembly.
These carbide pieces were carefully fitted together on a machined-flat fixturing plate (that would go into the brazing furnace), with a temporary frame around it to keep all the segments closely aligned into a circular disc with tight joints. A thin piece of ceramic cloth had been placed on the flat-fixture surface between the fixture and the carbide-pieces to make sure that the carbide pieces did not get brazed to the fixture!
The BFM (BNi-2) foil we used was available to us in 4-inch wide (100mm) strips, approximately 0.002” (0.05mm) thick. We placed several foil strips side-by-side to cover the full diameter of the carbide circular-disc, and then placed a second layer of that foil on top of that, but with the sheets laid at a 90-degree angle to the first layer, as shown in Fig. 2.
On top of this we then placed an 18-in (45 cm) diameter disc of the pure Nickel-200, approximately 5/64” (2mm) thick, to act as a “shock absorber” for the stresses that would be created between the carbide and tool steel during the high-temp nickel-brazing process.
Then, on top of the thick Nickel-200 layer we placed two more layers of the BNi-2 foil, in the same lay-up manner as we did below the Nickel-200 layer, and finally, carefully laid the tool-steel die on top of that. The die would essentially be then acting as a “dead weight” on top of the vertical assembly, pushing all the layers tightly together. As can be readily seen in Fig. 2, we were essentially nickel-brazing the carbide-disc to the ductile nickel-core from one side, and nickel-brazing the tool steel die to the ductile nickel-core from the other side. We wanted that layer of pure-nickel (Nickel-200) to be thick enough so that the diffusion of the BFM into that layer from each side would be minimal since we wanted most of that pure-nickel sheet to remain un-alloyed and as ductile as possible for its “shock-absorbing” purposes.
We carefully aligned all pieces vertically, and then placed two (2) spring-loaded ring pieces around the base of the stacked assembly, tall enough to cover the brazed joint stack-up and a little of the die itself. The surfaces of that spring-loaded fixture were painted with brazing “stop-off” to prevent sticking of the fixture to the stacked assembly being brazed. The Inconel springs allowed the assembly to grow (expand) outward during heating, but kept constant pressure on the stack, even during cooling as the brazed assembly began to contract (shrink) back to its original size.
Thermocouples were placed into holes already drilled into the open side of the die, so they could read temps inside the die very near to the joint-interface between the die and the Nickel-200 layer. We brazed in a vacuum furnace at about 1950F (1065C), which was a little more than 100F (50C) above the liquidus temp for that BNi-2 BFM, meaning that when that brazing-temp (1950F) was reached, the BFM should indeed have fully flowed! We held the furnace at that temp until all the deeply embedded load-TC’s had reached that brazing temp and stayed there for only a few minutes (5-minutes max), since dwelling at brazing temp too long would have allowed the BFM to diffuse too deeply into the ductile Nickel-200 layer, thereby hardening that layer so much that it couldn’t effectively act as a “shock-absorber”.
We then VERY SLOWLY lowered the temp in the furnace (we did NOT merely turn off the vacuum furnace) since we did not want to cause any significant temp-differentials anywhere in the brazed assembly that might cause the carbides to distort or crack. This is ALWAYS very important when brazing carbides or any other metal combinations in which there are significant differences in the COE’s between the two materials being joined.
The front face of the brazed carbide assembly was carefully inspected after brazing, and the BNi-2 BFM had flowed well into all the thin joints between each of the carbide pie-segments. Following inspection, the surface of the brazed carbide disc was processed to a very smooth finish, holes were put into and through the brazed die assembly, and when placed in service, it performed very well for its intended life.
CONCLUSIONS: Brazing can be used to very effectively join materials together that have widely different Coefficients Of Thermal Expansion (COE’s), even when the parts being joined are very large. The design of the joint is very important, and the judicious use of “shock absorber” layers should be considered. Of equal importance is the actual furnace brazing cycle used. It is very, very important that such assemblies be very slowly heated up to brazing temp, using a number of buried TC’s to verify that the temps at different locations inside the assembly are kept quite close together throughout the entire heating and cooling cycles. Otherwise, when large delta-T’s, i.e., temp differentials, occur in such assemblies, it inevitably can lead to distortion or cracking of the assembly. Let me stress again (pun intended) that after the assembly has briefly soaked at brazing temp, it MUST be very slowly cooled back down to room temp to avoid distortion or cracking.
Thus, when the joint design has been properly made, and the brazing cycle is properly controlled, you can have a high degree of confidence that brazing will give you the superb results you want.
Dan Kay – Tel: (860) 651-5595 – Dan Kay operates his own brazing consulting/training company, and has been involved full-time in brazing for 50-years. Dan regularly consults in areas of vacuum and atmosphere brazing, as well as in torch (flame) and induction brazing. His brazing seminars, held a number of times each year to help people learn how to apply the fundamentals of brazing to improve their productivity and lower their costs. Dan can be reached via e-mail at email@example.com, and his website can be visited at http://www.kaybrazing.com/
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