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Archives for March 2015

Maintaining Oil Diffusion Pumps

March 10, 2015 by VAC AERO International

Maintaining Oil Diffusion Pumps

Even as turbomolecular vacuum pumps have displaced most small laboratory sized oil diffusion pumps these days because of perceived ease of use and cleanliness, most high vacuum heat treating furnaces still rely on a large oil diffusion pumps to generate the pressures below about 10-3 Torr needed for many metal conditioning processes.

The main reason for this is that turbomolecular vacuum pumps have a physical size limit due to the high rotational speed of the rotor. That size limit is around 320 mm or 13 inches inlet diameter and may vary a small amount from manufacturer to manufacturer. In many cases the pumping speed may not be high enough as it is directly related to the inlet size of the pump. Metal can disintegrate at very high speed, so the tip speed of the rotor blades has to be within the safe limit. Turbomolecular pump rotors have to move faster than the speed of the gas molecules they are pumping in order that the rotor blades can deflect the gas molecules downwards in the pump mechanism. The second reason that turbomolecular pumps are not used in many metal treating systems is they cannot tolerate any particulate matter entering them. They must only be used on clean vacuum systems.

Metallographic Imaging Modes

March 1, 2015 by George Vander Voort

5 wsThe reflected light microscope is the most commonly used tool for the study of the microstructure of metals. It has long been recognized that the microstructure of metals and alloys has a profound influence on many of their properties. Mechanical properties (strength, toughness, ductility, etc.) are influenced much more than physical properties (many are insensitive to microstructure).

The structure of metals and alloys can be viewed at a wide range of levels – macrostructure, microstructure, and ultra-microstructure. Microstructural examination should always begin with the light microscope progressing from low magnifications to higher magnifications, followed by the use of electron instruments, as needed. In the study of microstructure, the metallographer determines what phases or constituents are present, their relative amounts, and their size, spacing, morphology and arrangement. The microstructure is established based upon the chemical composition of the alloy and the processing steps. A small specimen is cut from a larger mass (for example: a casting, forging, rolled bar, plate, sheet, or wire) for evaluation.

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