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Archives for December 2013

A Brief History of Vacuum Technology

December 15, 2013 by Dan Herring

A Brief History of Vacuum Technology

The history of vacuum technology is a fascinating one. It seems to have begun in ancient Greece when the philosopher Democritus (circa 460 to 375 B.C.) proposed that the world was made up of tiny particles that he called atoms (atomos, Greek: undividable). Democritus proposed that empty space (in other words, in modern terminology, a vacuum) existed between the atoms, which moved according to the general laws of mechanics. Democritus, together with his teacher Leucippus, may be considered as the inventors of the concept of a vacuum. Our modern view of physics is heavily influenced by the ideas of Democritus.

However, it was the thinking of Aristotle (384 – 322 B.C.) that dominated the scientific community up until the 16th century. Aristotle denied the existence of a vacuum as it conflicted with the idea that the universe was comprised of countless individual particles. According to Aristotle, nature consisted of the four basic elements namely water, earth, air, and fire.  In fact, the word vacuum comes to us from the Latin word “vacuus” meaning empty or “vacare” meaning “to be empty”.

A Curious Case of Part Contamination in a Vacuum Furnace

December 14, 2013 by Dan Herring

A Curious Case of Part Contamination in a Vacuum Furnace

A manufacturer of quartz products for the lighting industry was curious as to the origin of black “flakes” (particles) found on the outside and inside surfaces of their quartz tubes after heat treatment. These flakes appeared to be “fluffy bits of carbon”. The thought process to investigate this phenomenon presents a unique learning experience for us all.

One of the last steps of the quartz-production process is the heat treatment of the quartz tubes, which takes place in one of several vacuum furnaces at this manufacturer’s facility. The quartz tubes are heated under vacuum to 1050°C (1220°F) and held at temperature for several hours. This is followed by a quench with nitrogen. The vacuum furnaces in question have graphite heating elements, a combination ceramic fiber/felt insulation pack with a molybdenum hot face and stainless steel cold face and a graphite hearth. The quartz tubes themselves are placed onto graphite fixtures (racks).

Obtaining Consistent Vickers Hardness at Loads ≤ 100 Grams Force

December 6, 2013 by George Vander Voort

Obtaining Consistent Vickers Hardness at Loads ≤ 100 Grams Force

One of the most serious limitations to Vickers hardness testing in the micro-load range (10-1000 gf or 0.098-9.81 N) has been the variability in measured hardness with loads ≤ 100 gf (≤ 0.98 N). In the literature four HV-load trends have been reported for this range.  In the order of most common to least common, the trends are: the hardness decreases with decreasing load; the hardness increases slightly and then decreases; the hardness increases with decreasing load; and, the hardness is constant. Many publications have concentrated on the most common trend and attributed it to material factors. Samuels [1] stated, however, that these problems were due to microscope limitations, such as limited contrast and resolution, and visual perception limitations. At the same symposium, Westrich [2] showed that the SEM could be used to measure small Vickers indents and yield virtually constant hardness as a function of load.

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